OBJECTIVE: To study on the phlorotannins in Ecklonia kurome. METHODS: Silica gel column chromatography and Sephadex LH-20 column chromatography were conducted for isolation and identification of phlorotannins, and the compound structures were analyzed and identified based on physicochemical properties and spectral data. RESULTS: Totally 7 phlorotannins were isolated from E. kurome, namely Phloroglucinol (1),Eckol (2), Fucodiphloroethol G(3), Phlorofucofuroeckol A (4), 1-(3′ ,5′ -dihydro-xyphenoxy)-7-(2″ ,4″ ,6-trihydro-xyphenoxy)-2,4,9-trihydroxydibenzo-1,4-dioxin (5),Dieckol (6) and 6,6′ -bieckol (7). CONCLUSIONS: Compound 5 and 7 are isolated from E. kurome for the first time, and the study has laid a foundation for its quality evaluation.
关键词
昆布提取分离聚合酚类成分结构鉴定
Keywords
Ecklonia kuromeExtraction and isolationPhlorotanninsStructure identification