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天津中医药大学中药学院/天津市中药化学与分析重点实验室,天津 301600
硕士研究生。研究方向:中药炮制、中药质量控制。E-mail:Ftc0190@163.com
教授,硕士生导师,博士。研究方向:中药炮制、中药质量控制。E-mail:zhiyingdou@163.com
纸质出版日期:2022-11-30,
收稿日期:2022-04-15,
修回日期:2022-10-09,
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范天慈,毛睿,刘丽婷等.基于多指标成分含量的酒萸肉干燥方式研究 Δ[J].中国药房,2022,33(22):2724-2727.
FAN Tianci,MAO Rui,LIU Liting,et al.Study on the drying methods of wine-processed Cornus officinalis based on the contents of multi-index components[J].ZHONGGUO YAOFANG,2022,33(22):2724-2727.
范天慈,毛睿,刘丽婷等.基于多指标成分含量的酒萸肉干燥方式研究 Δ[J].中国药房,2022,33(22):2724-2727. DOI: 10.6039/j.issn.1001-0408.2022.22.07.
FAN Tianci,MAO Rui,LIU Liting,et al.Study on the drying methods of wine-processed Cornus officinalis based on the contents of multi-index components[J].ZHONGGUO YAOFANG,2022,33(22):2724-2727. DOI: 10.6039/j.issn.1001-0408.2022.22.07.
目的
2
考察不同干燥方式对酒萸肉中指标成分的影响,以优选最佳干燥方式。
方法
2
山萸肉饮片经酒制后,分别采用不同干燥方式(鼓风干燥、远红外干燥、微波干燥、冷冻干燥、晒干、阴干及联合干燥)进行干燥。采用高效液相色谱法测定酒萸肉中没食子酸等5种成分的含量;采用显色法测定酒萸肉中总黄酮的含量;采用层次分析法评价不同干燥方式对酒萸肉成分含量的影响。
结果
2
22批酒萸肉中没食子酸、5-羟甲基糠醛、莫诺苷、马钱苷、山茱萸新苷、总黄酮的含量分别为1.043 8~1.563 8、0.648 5~2.358 8、5.031 0~10.305 7、6.681 2~7.534 2、0.986 5~1.148 8、33.657 2~50.741 5 mg/g。层次分析法综合评价结果显示,75 ℃微波干燥时酒萸肉中各成分的综合评分最高,其次为60 ℃鼓风干燥和60 ℃远红外干燥所得样品。
结论
2
酒萸肉的干燥方式宜采用75 ℃微波干燥、60 ℃鼓风干燥或60 ℃远红外干燥。
OBJECTIVE
2
To investigate the effects of different drying methods on the index components in wine-processed
Cornus officinalis
so as to optimize drying method.
METHODS
2
After processed with wine,
C. officinalis
decoction pieces were dried with different drying methods (blast drying, far infrared drying, microwave drying, freeze drying, sun drying, shade drying and combined drying). The contents of 5 components such as gallic acid in wine-processed
C. officinalis
were determined by high-performance liquid chromatography. The contents of total flavonoids in wine-processed
C. officinalis
were determined by chromogenic method. Analytic hierarchy process was used to evaluate the effects of different drying methods on the contents of components in
C. officinalis
.
RESULTS
2
The contents of gallic acid, 5-hydroxymethylfurfural, monoside, loganin, cornuside and total flavonoids in 22 batches of wine-processed
C. officinalis
were 1.043 8-1.563 8, 0.648 5-2.358 8, 5.031 0-10.305 7, 6.681 2-7.534 2, 0.986 5-1.148 8 and 33.657 2-50.741 5 mg/g, respectively. The comprehensive scoring results of analytic hierarchy process showed that the comprehensive score of each component in
C. officinalis
dried by microwave at 75 ℃ was higher, followed by blast drying at 60 ℃ and far infrared drying at 60 ℃.
CONCLUSIONS
2
The wine-processed
C. officinalis
could be dried by microwave drying at 75 ℃, blast drying at 60 ℃ or far infrared drying at 60 ℃.
酒萸肉干燥方式含量测定综合评价
drying methodcontent determinationcomprehensive evaluation
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